[4-(2,2':6',2''-TERPYRIDIN-4'-YL)PHENYL]METHANOL

Base Information

Chemical Name:[4-(2,2':6',2''-TERPYRIDIN-4'-YL)PHENYL]METHANOL
CAS No.:447399-94-2
Molecular Formula:C22H17N3O
Molecular Weight:339.396
Hs Code.:
Mol file:447399-94-2.mol

Synonyms:4'-(4-Hydroxymethylphenyl)-2,2':6',2''-terpyridine;[4-(2,2':6',2''-Terpyridin-4'-yl)phenyl]methanol;

Suppliers and Price of [4-(2,2':6',2''-TERPYRIDIN-4'-YL)PHENYL]METHANOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 8 raw suppliers

Chemical Property of [4-(2,2':6',2''-TERPYRIDIN-4'-YL)PHENYL]METHANOL

Chemical Property:

Boiling Point:535.9 °C at 760 mmHg
Flash Point:277.9 °C
PSA：58.90000
Density:1.217 g/cm³
LogP:4.36490

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of [4-(2,2':6',2''-TERPYRIDIN-4'-YL)PHENYL]METHANOL

There total 5 articles about [4-(2,2':6',2''-TERPYRIDIN-4'-YL)PHENYL]METHANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1122-62-9
2-acetylpyridine

: 52010-97-6
4-(hydroxylmethyl)benzaldehyde

: 447399-94-2
4′-(4-hydroxymethylphenyl)-2,2′:6′,2′′-terpyridine

Guidance literature:: 2-acetylpyridine; 4-(hydroxylmethyl)benzaldehyde; With sodium hydroxide; at 0 ℃; for 2h;

With ammonia; In water; at 100 ℃; for 2h;
DOI:10.1039/c3ob40620b

Reference yield:

: C₂₂H₂₀N₂O₃

: 447399-94-2
4′-(4-hydroxymethylphenyl)-2,2′:6′,2′′-terpyridine

Guidance literature:: With ammonium hydroxide; In various solvent(s); at 100 ℃; for 2h;
DOI:10.1055/s-2006-942525

Reference yield:

: 623-27-8
terephthalaldehyde,

: 447399-94-2
4′-(4-hydroxymethylphenyl)-2,2′:6′,2′′-terpyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C

2.1: sodium hydroxide / 2 h / 0 °C

2.2: 2 h / 100 °C

With sodium tetrahydroborate; sodium hydroxide; In tetrahydrofuran;
DOI:10.1039/c3ob40620b