tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate

Base Information

Chemical Name:tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate
CAS No.:1643719-03-2
Molecular Formula:C₃₄H₄₉NO₆
Molecular Weight:567.766
Hs Code.:

Synonyms:tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate

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Chemical Property of tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate

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Technology Process of tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate

There total 9 articles about tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 14267-92-6
1-chloro-4-pentyne

: 1643719-02-1
tert-butyl-N-6-{4-[6-(4-hydroxyphenyloxy)hexyloxy]phenyloxy}-hexylcarbamate

: 1643719-03-2
tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate

Guidance literature:: tert-butyl-N-6-{4-[6-(4-hydroxyphenyloxy)hexyloxy]phenyloxy}-hexylcarbamate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h; Inert atmosphere;

1-chloro-4-pentyne; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1002/ejoc.201402249

Reference yield:

: 56219-56-8
1-(benzyloxy)-4-(6-bromohexyloxy)benzene

: 1643719-03-2
tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

1.2: 48 h / 20 °C / Inert atmosphere

2.1: hydrogen; palladium 10% on activated carbon / chloroform / 23 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

3.2: 18 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; sodium hydride; In chloroform; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201402249

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 1643719-03-2
tert-butyl-N-6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / 21 h / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

2.2: 48 h / 20 °C / Inert atmosphere

3.1: hydrogen; palladium 10% on activated carbon / chloroform / 23 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

4.2: 18 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; sodium hydride; potassium carbonate; In chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1002/ejoc.201402249