1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate

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Chemical Name:1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate
CAS No.:1224950-02-0
Molecular Formula:C₂₅H₂₆N₂O₄
Molecular Weight:418.492
Hs Code.:

Synonyms:1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate

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Chemical Property of 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate

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Technology Process of 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate

There total 10 articles about 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1224949-08-9
c-4-hydroxy-1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cyclohexan-r-1-yl acetate

: 1224950-02-0
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 70097-74-4
8-ethynyl-1,4-dioxaspiro[4.5]decan-8-ol

: 1224950-02-0
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.92 h / -72 °C

1.2: 0.58 h / -72 °C

2.1: manganese(IV) oxide / dichloromethane / 15 h / 20 °C

3.1: triethylamine / ethanol / 0.5 h / 20 °C

3.2: 15 h / 20 °C

4.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

4.2: 0 °C

5.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

6.1: dmap; pyridine / dichloromethane / 66 h / 20 °C

7.1: potassium carbonate; methanol / 4 h / 20 °C

8.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C

With pyridine; hydrogenchloride; methanol; dmap; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; water; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1224950-02-0
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-4-oxo-cyclohexan-1-yl acetate

Guidance literature:: Multi-step reaction with 10 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -76 °C

1.2: 2 h / -74 °C

2.1: potassium carbonate; methanol / 2 h / 20 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.92 h / -72 °C

3.2: 0.58 h / -72 °C

4.1: manganese(IV) oxide / dichloromethane / 15 h / 20 °C

5.1: triethylamine / ethanol / 0.5 h / 20 °C

5.2: 15 h / 20 °C

6.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

6.2: 0 °C

7.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

8.1: dmap; pyridine / dichloromethane / 66 h / 20 °C

9.1: potassium carbonate; methanol / 4 h / 20 °C

10.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C

With pyridine; hydrogenchloride; methanol; dmap; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; water; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane;