2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone

Base Information

Chemical Name:2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone
CAS No.:125744-09-4
Molecular Formula:C₁₅H₁₄N₂O₅S
Molecular Weight:334.353
Hs Code.:

Synonyms:2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone

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Chemical Property of 2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone

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Technology Process of 2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone

There total 4 articles about 2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.6%

: 100-00-5
4-chlorobenzonitrile

: 125744-08-3
4-acetamino-2-methyl-benzenesulfinic acid

: 125744-09-4
2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 95 ℃;

Reference yield:

: 133-78-8
4-amino-2-methylbenzenesulphonic acid

: 125744-09-4
2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone

Guidance literature:: Multi-step reaction with 4 steps

1: 66.4 percent

2: SOCl₂ / dimethylformamide / 0.17 h

3: Na₂SO₃ / H₂O / 0.17 h

4: 64.6 percent / NaH / dimethylformamide / 95 °C

With thionyl chloride; sodium hydride; sodium sulfite; In water; N,N-dimethyl-formamide;

Reference yield:

: 62374-67-8
4-acetamino-2-methyl-benzenesulfonyl chloride

: 125744-09-4
2-methyl-4-acetylamino-4'-nitrodiphenyl sulphone

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂SO₃ / H₂O / 0.17 h

2: 64.6 percent / NaH / dimethylformamide / 95 °C

With sodium hydride; sodium sulfite; In water; N,N-dimethyl-formamide;