triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane

Base Information

Chemical Name:triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane
CAS No.:876032-08-5
Molecular Formula:C₂₃H₄₆O₂Si₂
Molecular Weight:410.788
Hs Code.:

Synonyms:triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane

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Chemical Property of triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane

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Technology Process of triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane

There total 2 articles about triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: lithium (E)-di[4-triisopropylsilyloxy]-2-butenylcupurate

: 54307-74-3,15466-88-3
(R)-5-methyl-cyclohex-2-enone

: 876032-08-5
triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane

Guidance literature:: In tetrahydrofuran; at -40 ℃; for 1h;

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 1185583-57-6
(E)-3-tributylstannyl-2-butenyl triisopropyl silyl ether

: 54307-74-3,15466-88-3
(R)-5-methyl-cyclohex-2-enone

: 876032-08-5
triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane

Guidance literature:: (E)-3-tributylstannyl-2-butenyl triisopropyl silyl ether; With n-butyllithium; In tetrahydrofuran; hexane; at -40 - -30 ℃; Inert atmosphere;

With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; hexane; at -40 ℃; for 0.5h; Inert atmosphere;

chloro-trimethyl-silane; (R)-5-methyl-cyclohex-2-enone; In tetrahydrofuran; hexane; at -40 ℃; Inert atmosphere;
DOI:10.1002/chem.200900310

Reference yield:

: 876032-08-5
triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane

: 439588-93-9
5-(tert-butyldimethylsilyl)-4-methylfuran-2-carbaldehyde

: 876032-09-6
C₃₂H₅₈O₄Si₂

: 876032-21-2
C₃₂H₅₈O₄Si₂

Guidance literature:: triisopropyl-((E)-3-((1R,5R)-5-methyl-3-(trimethylsilyloxy)cyclohex-2-enyl)but-2-enyloxy)silane; With n-butyllithium; In tetrahydrofuran; at -30 ℃; for 2h;

With zinc dibromide; In tetrahydrofuran; at -78 ℃; for 2h;

5-(tert-butyldimethylsilyl)-4-methylfuran-2-carbaldehyde; In tetrahydrofuran; at -78 ℃; for 3h;