1-((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-4-methyl[(2-methylpiperidinyl)diazen-1-ium-1,2-diol-2-ate]

Base Information

Chemical Name:1-((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-4-methyl[(2-methylpiperidinyl)diazen-1-ium-1,2-diol-2-ate]
CAS No.:1609067-95-9
Molecular Formula:C₁₉H₃₀BN₃O₄
Molecular Weight:375.276
Hs Code.:

Synonyms:1-((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-4-methyl[(2-methylpiperidinyl)diazen-1-ium-1,2-diol-2-ate]

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Chemical Property of 1-((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-4-methyl[(2-methylpiperidinyl)diazen-1-ium-1,2-diol-2-ate]

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Technology Process of 1-((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-4-methyl[(2-methylpiperidinyl)diazen-1-ium-1,2-diol-2-ate]

There total 1 articles about 1-((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-4-methyl[(2-methylpiperidinyl)diazen-1-ium-1,2-diol-2-ate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 428866-71-1
C₆H₁₂N₃O₂^(1-)*Na⁽¹⁺⁾

: 138500-85-3
4-bromomethylphenylboronic acid pinacol ester

: 1609067-95-9
1-((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-4-methyl[(2-methylpiperidinyl)diazen-1-ium-1,2-diol-2-ate]

Guidance literature:: C₆H₁₂N₃O₂^(1-)*Na⁽¹⁺⁾; With 15-crown-5; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere;

4-bromomethylphenylboronic acid pinacol ester; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol5010643

Reference yield:

: 1609067-95-9
1-((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-4-methyl[(2-methylpiperidinyl)diazen-1-ium-1,2-diol-2-ate]

: 10102-43-9
nitrogen(II) oxide

Guidance literature:: With dihydrogen peroxide; acetic acid; In aq. phosphate buffer; water; dimethyl sulfoxide; at 37 ℃; pH=7.4;
DOI:10.1021/ol5010643