4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal

Base Information

Chemical Name:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal
CAS No.:943239-68-7
Molecular Formula:C₁₅H₂₃BO₄
Molecular Weight:278.156
Hs Code.:

Synonyms:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal

Suppliers and Price of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal

There total 8 articles about 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 24856-58-4
1,1-dimethoxy-1-(4-bromophenyl)methane

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 943239-68-7
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal

Guidance literature:: With iodine; magnesium; In tetrahydrofuran; at 25 ℃; Inert atmosphere;
DOI:10.1021/jo201093u

Reference yield: 81.0%

: 943239-68-7
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal

Guidance literature:: With iodine; magnesium; In tetrahydrofuran; at 25 ℃; for 3.083h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; at 0 - 25 ℃; for 0.666667h;

Reference yield: 76.0%

: 100515-17-1
1-(1,1-dimethoxy-methyl)-4-methylsulfanyl-benzene

: 73183-34-3
bis(pinacol)diborane

: 943239-68-7
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzaldehydedimethyl acetal

Guidance literature:: With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; lithium hexamethyldisilazane; In tetrahydrofuran; at 80 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.6b01305