(R)-3-vinylcyclohex-2-enyl acetate

Base Information

Chemical Name:(R)-3-vinylcyclohex-2-enyl acetate
CAS No.:1497432-46-8
Molecular Formula:C₁₀H₁₄O₂
Molecular Weight:166.22
Hs Code.:

Synonyms:(R)-3-vinylcyclohex-2-enyl acetate

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Chemical Property of (R)-3-vinylcyclohex-2-enyl acetate

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Technology Process of (R)-3-vinylcyclohex-2-enyl acetate

There total 3 articles about (R)-3-vinylcyclohex-2-enyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 7486-35-3
tri-n-butyl(vinyl)tin

: (R)-3-iodocyclohex-2-en-1-yl acetate

: 1497432-46-8
(R)-3-vinylcyclohex-2-enyl acetate

Guidance literature:: With copper(l) iodide; triphenyl-arsane; palladium diacetate; In acetone; at 50 ℃; for 0.333333h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jo402086z

Reference yield:

: 188635-27-0
3-iodo-2-cyclohexen-1-ol

: 1497432-46-8
(R)-3-vinylcyclohex-2-enyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; dicarbonyl(chloro)(η⁵-pentaphenylcyclopentadienyl)ruthenium(II); potassium tert-butylate / tetrahydrofuran; toluene / 24 h / 30 °C / Inert atmosphere; Schlenk technique; Enzymatic reaction

2: palladium diacetate; copper(l) iodide; triphenyl-arsane / acetone / 0.33 h / 50 °C / Inert atmosphere; Microwave irradiation

With copper(l) iodide; dicarbonyl(chloro)(η⁵-pentaphenylcyclopentadienyl)ruthenium(II); triphenyl-arsane; potassium tert-butylate; palladium diacetate; sodium carbonate; In tetrahydrofuran; acetone; toluene; 2: |Stille Cross Coupling;
DOI:10.1021/jo402086z

Reference yield:

: 56671-82-0
3-Iodocyclohex-2-enone

: 1497432-46-8
(R)-3-vinylcyclohex-2-enyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: cerium(III) chloride heptahydrate; sodium tetrahydroborate; ammonium chloride / methanol; water / 3 h / 0 °C

2: sodium carbonate; dicarbonyl(chloro)(η⁵-pentaphenylcyclopentadienyl)ruthenium(II); potassium tert-butylate / tetrahydrofuran; toluene / 24 h / 30 °C / Inert atmosphere; Schlenk technique; Enzymatic reaction

3: palladium diacetate; copper(l) iodide; triphenyl-arsane / acetone / 0.33 h / 50 °C / Inert atmosphere; Microwave irradiation

With sodium tetrahydroborate; copper(l) iodide; dicarbonyl(chloro)(η⁵-pentaphenylcyclopentadienyl)ruthenium(II); triphenyl-arsane; cerium(III) chloride heptahydrate; potassium tert-butylate; palladium diacetate; sodium carbonate; ammonium chloride; In tetrahydrofuran; methanol; water; acetone; toluene; 3: |Stille Cross Coupling;
DOI:10.1021/jo402086z