C₁₀H₉⁽²⁾H₂Cl

Base Information

• Chemical Name: C₁₀H₉⁽²⁾H₂Cl
• CAS No.: 70576-42-0
• Molecular Formula: C₁₀H₁₁Cl
• Molecular Weight: 168.634
• Mol file: 70576-42-0.mol

Synonyms:C₁₀H₉⁽²⁾H₂Cl

Chemical Property of C₁₀H₉⁽²⁾H₂Cl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₉⁽²⁾H₂Cl

There total 6 articles about C₁₀H₉⁽²⁾H₂Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-phenyl-2-methylprop-2-en-1-ol-1,1-d2 (70576-41-9) → C10H9(2)H2Cl (70576-42-0)

Guidance literature:

With N-chloro-succinimide; dimethylsulfide; In dichloromethane; at -40 - 20 ℃;

DOI:10.1021/jo9715332

Reference yield:

(E)-methyl-2-methyl-3-phenylacrylate (22946-43-6) → C10H9(2)H2Cl (70576-42-0)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlD₄; AlCl₃

2: NCS; Me₂S

With N-chloro-succinimide; aluminium trichloride; lithium aluminium deuteride; dimethylsulfide;

DOI:10.1021/jo026198i

Reference yield:

2-methyl-3-phenylacrylic acid (1895-97-2) → C10H9(2)H2Cl (70576-42-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 3.2 g / p-TsOH / Heating

2: LiAlD₄, AlCl₃ / 0 h / 0 °C

3: 2.2 g / NCS, Me₂S / CH₂Cl₂ / -40 - 20 °C

With N-chloro-succinimide; aluminium trichloride; lithium aluminium deuteride; dimethylsulfide; toluene-4-sulfonic acid; In dichloromethane;

DOI:10.1021/jo9715332

upstream raw materials:

(E)-3-phenyl-2-methylprop-2-en-1-ol-1,1-d2

(E)-methyl-2-methyl-3-phenylacrylate

benzaldehyde

2-methyl-3-phenylacrylic acid

Downstream raw materials:

[(E)-2-methyl-3,3,3-trideuterio-1-propenyl]benzene