C₁₇H₂₃NO₃

Base Information

Chemical Name:C₁₇H₂₃NO₃
CAS No.:1280201-27-5
Molecular Formula:C₁₇H₂₃NO₃
Molecular Weight:289.375
Hs Code.:

C<sub>17</sub>H<sub>23</sub>NO<sub>3</sub>

Synonyms:C₁₇H₂₃NO₃

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Chemical Property of C₁₇H₂₃NO₃

Chemical Property:

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Technology Process of C₁₇H₂₃NO₃

There total 5 articles about C₁₇H₂₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1280201-06-0
1-(2,6-dimethylphenyl)-3-ethyl-5-oxo-pyrrolidine-3-carboxylic acid methyl ester

: 74-88-4
methyl iodide

: 1280201-27-5
C₁₇H₂₃NO₃

Guidance literature:: 1-(2,6-dimethylphenyl)-3-ethyl-5-oxo-pyrrolidine-3-carboxylic acid methyl ester; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.333333h;

methyl iodide; In tetrahydrofuran; at -78 - 20 ℃; for 1h;

Reference yield:

: 97-65-4,25119-64-6
2-methylenesuccinic acid

: 1280201-27-5
C₁₇H₂₃NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 0.75 h / 130 °C

2.1: acetyl chloride / 1 h / 64 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / -50 - 0 °C

3.2: 2 h / -50 - 20 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 °C

4.2: 1 h / -78 - 20 °C

With acetyl chloride; lithium hexamethyldisilazane; In tetrahydrofuran;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 1280201-27-5
C₁₇H₂₃NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 0.75 h / 130 °C

2.1: acetyl chloride / 1 h / 64 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / -50 - 0 °C

3.2: 2 h / -50 - 20 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 °C

4.2: 1 h / -78 - 20 °C

With acetyl chloride; lithium hexamethyldisilazane; In tetrahydrofuran;