phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside

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Chemical Name:phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside
CAS No.:1283073-28-8
Molecular Formula:C₃₆H₃₉N₃O₇S
Molecular Weight:657.788
Hs Code.:

Synonyms:phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 824-94-2
p-methoxybenzyl chloride

: 166516-67-2
phenyl 2-azido-2-deoxy-1-thio-β-D-glucopyranoside

: 1283073-28-8
phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside

Guidance literature:: phenyl 2-azido-2-deoxy-1-thio-β-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/jo102411j

Reference yield: 94.0%

: 1283073-28-8
phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: phenyl 2-deoxy-3,4,6-tri-O-p-methoxybenzyl-1-thio-2-N-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside; With acetic acid; zinc; In 1,4-dioxane; at 0 - 20 ℃; for 24h;

With sodium hydrogencarbonate; In 1,4-dioxane; water; for 0.25h;

2,2,2-Trichloroethyl chloroformate; In 1,4-dioxane; water; at 20 ℃; for 24h;
DOI:10.1002/chem.201605627