1-Propionylethyl acetate

Base Information

• Chemical Name: 1-Propionylethyl acetate
• CAS No.: 2983-05-3
• Molecular Formula: C7H12 O3
• Molecular Weight: 144.17
• Mol file: 2983-05-3.mol

Synonyms:3-Pentanone,2-hydroxy-, acetate (6CI,8CI)

Chemical Property of 1-Propionylethyl acetate

Chemical Property:

• PSA: 43.37000
• LogP: 0.91710

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Propionylethyl acetate

There total 2 articles about 1-Propionylethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.6%

3,3-dimethyldioxirane (74087-85-7) + pentan-3-one (96-22-0) → Acetol acetate (592-20-1) + 1-methyl-2-oxobutyl acetate (2983-05-3)

Guidance literature:

In acetone; Yields of byproduct given; Heating;

DOI:10.1021/jo00041a036

Reference yield:

3-pentanone oxime (1188-11-0) + acetyl chloride (75-36-5) → 1-methyl-2-oxobutyl acetate (2983-05-3) + pentan-3-one (96-22-0)

Guidance literature:

With tertiary base; water; In acetic anhydride; Heating; 1.) 4 h, 2.) 30 min;

DOI:10.1055/s-1981-29394

upstream raw materials:

3-pentanone oxime

acetyl chloride

3,3-dimethyldioxirane

pentan-3-one

Refernces

• 1、 Reddy, Gaddam Subba,Bhatt, M. Vivekananda. "A New One-Step Conversion of Ketoximes into α-Acyloxyketones". . p. 223 - 224. Retrieved 2007/10/02.