cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]

Base Information

Chemical Name:cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]
CAS No.:876061-92-6
Molecular Formula:C₂₂H₂₇Cl₂N₃Pd
Molecular Weight:510.802
Hs Code.:

cis-[PdCl<sub>2</sub>(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]

Synonyms:cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]

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Chemical Property of cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]

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Technology Process of cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]

There total 1 articles about cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 192711-31-2
2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)-pyridine

: 876061-92-6
cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]

Guidance literature:: In acetonitrile; using Schlenk techniques; dissolving of 2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine in dry MeCN; addn. to soln. of PdCl2(MeCN)2 in dry MeCN; stiring at room temp. for 10 h; concn., pptn., recrystn. in acetone; filtration, washing with diethyl ether; drying in vac., elem. anal.;
DOI:10.1016/j.ica.2005.07.047

Reference yield: 85.0%

: 110-86-1
pyridine

: 876061-92-6
cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]

: 143-66-8
sodium tetraphenyl borate

: cis-[Pd(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)(pyridine)2](BPh₄)2

Guidance literature:: With AgBF₄; In methanol; dichloromethane; byproducts: AgCl; using Schlenk techniques; dissolving of PdCl2(C3HN2(octyl)Ph(C5H4N)) in CH2Cl2/MeOH (3:1); addn. of py and then soln. of AgBF4 in MeOH; stirringat room temp. for 5 min in the dark; filtration, stirring for 1 h; conc n. in vac., addn. of NaBPh4; pptn., filtration, washing in Et2O, drying in vac.; elem. anal.;
DOI:10.1016/j.ica.2005.07.047

Reference yield: 51.0%

: 876061-92-6
cis-[PdCl₂(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)]

: 143-66-8
sodium tetraphenyl borate

: 603-35-0
triphenylphosphine

: cis-[Pd(2-(1-octyl-5-phenyl-1H-pyrazol-3-yl)pyridine)(triphenylphosphine)2](BPh₄)2

Guidance literature:: With AgBF₄; In methanol; dichloromethane; acetonitrile; byproducts: AgCl; using Schlenk techniques; dissolving of PdCl2(C3HN2(octyl)Ph(C5H4N)) in CH2Cl2, MeOH and MeCN; addn. of soln. AgBF4 in MeOH; stirring at room temp. for 5 min in the dark; addn. of PPh3; stirring for 6 h at room temp.; concn. in vac., addn. of NaBPh4; pptn., filtration, washing in Et2O, drying in vac.; elem. anal.;
DOI:10.1016/j.ica.2005.07.047