2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide

Base Information

Chemical Name:2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide
CAS No.:1195942-81-4
Molecular Formula:C₂₇H₂₈N₂O₄
Molecular Weight:444.53
Hs Code.:

Synonyms:2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide

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Chemical Property of 2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide

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Technology Process of 2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide

There total 6 articles about 2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₂₆ClNO₄

: 1195942-81-4
2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide

Guidance literature:: With ammonia; sodium hydrogencarbonate; In dichloromethane; water; ethyl acetate; at 20 ℃; for 1.5h;

Reference yield:

: 199330-64-8
2-amino-indane-2-carboxylic acid methyl ester hydrochloride

: 1195942-81-4
2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / dichloromethane; water; ethyl acetate / 0.5 h / 20 °C

2: water; lithium hydroxide / 1,4-dioxane / 0.5 h / 60 °C

3: thionyl chloride / 0.5 h / 60 °C

4: ammonia; sodium hydrogencarbonate / dichloromethane; water; ethyl acetate / 1.5 h / 20 °C

With thionyl chloride; ammonia; water; sodium hydrogencarbonate; lithium hydroxide; In 1,4-dioxane; dichloromethane; water; ethyl acetate;

Reference yield:

: 1195944-88-7
4-methoxy-3-(2-m-tolyl-ethoxy)-benzoic acid

: 1195942-81-4
2-[4-methoxy-3-(2-m-tolyl-ethoxy)-benzoylamino]-indane-2-carboxylic acid amide

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 0.33 h / 60 °C

2: sodium hydrogencarbonate / dichloromethane; water; ethyl acetate / 0.5 h / 20 °C

3: water; lithium hydroxide / 1,4-dioxane / 0.5 h / 60 °C

4: thionyl chloride / 0.5 h / 60 °C

5: ammonia; sodium hydrogencarbonate / dichloromethane; water; ethyl acetate / 1.5 h / 20 °C

With thionyl chloride; ammonia; water; sodium hydrogencarbonate; lithium hydroxide; In 1,4-dioxane; dichloromethane; water; ethyl acetate;