(+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate

Base Information

Chemical Name:(+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate
CAS No.:1134635-21-4
Molecular Formula:C₂₀H₂₆N₂O₆
Molecular Weight:390.436
Hs Code.:

Synonyms:(+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate

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Chemical Property of (+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate

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Technology Process of (+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate

There total 1 articles about (+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1134635-20-3
(-)-methyl (S)-3-[4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate

: 106-95-6
allyl bromide

: 1134635-21-4
(+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate

Guidance literature:: (-)-methyl (S)-3-[4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate; With sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at -78 ℃; for 0.666667h; Inert atmosphere;

allyl bromide; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2008.11.043

Reference yield: 79.0%

: 75-77-4
chloro-trimethyl-silane

: 1134635-21-4
(+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate

: 1134635-22-5
(+)-(1S,2R,5S)-6-allyl-8-(2,4-dimethoxybenzyl)-2-methoxy-2-(trimethylsiloxy)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Guidance literature:: (+)-methyl (S)-3-[1-allyl-4-(2,4-dimethoxybenzyl)-3,6-dioxopiperazin-2-yl]propanoate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.666667h; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.bmc.2008.11.043