Technology Process of 6-amino-5-chloro-3,4-dimethoxybenzamide
There total 5 articles about 6-amino-5-chloro-3,4-dimethoxybenzamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iron; acetic acid;
at 105 ℃;
for 0.25h;
DOI:10.1071/CH9811561
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydrogen carbonate, potassium carbonate / H2O / 0.33 h / 70 - 80 °C
2: 52 percent / nitric acid / 0.25 h / 0 - 10 °C
3: 92 percent / 10percent aq. potassium permanganate / acetone / Heating
4: 1.) thionyl chloride, 2.) NH3 liq. / 1.) reflux, 2.) liquid nitrogen
5: 85 percent / Fe, acetic acid / 0.25 h / 105 °C
With
potassium permanganate; thionyl chloride; ammonia; nitric acid; iron; sodium hydrogencarbonate; potassium carbonate; acetic acid;
In
water; acetone;
DOI:10.1071/CH9811561
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 52 percent / nitric acid / 0.25 h / 0 - 10 °C
2: 92 percent / 10percent aq. potassium permanganate / acetone / Heating
3: 1.) thionyl chloride, 2.) NH3 liq. / 1.) reflux, 2.) liquid nitrogen
4: 85 percent / Fe, acetic acid / 0.25 h / 105 °C
With
potassium permanganate; thionyl chloride; ammonia; nitric acid; iron; acetic acid;
In
acetone;
DOI:10.1071/CH9811561
