(1R,5S,3Z)-1-[(R)-2-acetoxy-2-phenylacetoxy]-5-(N,N-dibenzylamino)-1-phenylhex-3-ene

Base Information

Chemical Name:(1R,5S,3Z)-1-[(R)-2-acetoxy-2-phenylacetoxy]-5-(N,N-dibenzylamino)-1-phenylhex-3-ene
CAS No.:155626-81-6
Molecular Formula:C₃₆H₃₇NO₄
Molecular Weight:547.694
Hs Code.:

Synonyms:(1R,5S,3Z)-1-[(R)-2-acetoxy-2-phenylacetoxy]-5-(N,N-dibenzylamino)-1-phenylhex-3-ene

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Chemical Property of (1R,5S,3Z)-1-[(R)-2-acetoxy-2-phenylacetoxy]-5-(N,N-dibenzylamino)-1-phenylhex-3-ene

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Technology Process of (1R,5S,3Z)-1-[(R)-2-acetoxy-2-phenylacetoxy]-5-(N,N-dibenzylamino)-1-phenylhex-3-ene

There total 2 articles about (1R,5S,3Z)-1-[(R)-2-acetoxy-2-phenylacetoxy]-5-(N,N-dibenzylamino)-1-phenylhex-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 51019-43-3
(R)-(-)-O-acetylmandelic acid

: 155626-76-9
(1R,5S,3Z)-5-(N,N-dibenzylamino)-1-phenylhex-3-en-1-ol

: 155626-81-6
(1R,5S,3Z)-1-[(R)-2-acetoxy-2-phenylacetoxy]-5-(N,N-dibenzylamino)-1-phenylhex-3-ene

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2012.05.032

Reference yield:

: 100-52-7
benzaldehyde

: 155626-81-6
(1R,5S,3Z)-1-[(R)-2-acetoxy-2-phenylacetoxy]-5-(N,N-dibenzylamino)-1-phenylhex-3-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: stannic bromide / dichloromethane / 0.17 h / -55 °C / Inert atmosphere

1.2: 1 h / -55 °C / Inert atmosphere

2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 18 h / 20 °C / Inert atmosphere

With dmap; stannic bromide; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tet.2012.05.032