(4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile

Base Information

• Chemical Name: (4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile
• CAS No.: 640732-63-4
• Molecular Formula: C₁₆H₁₅N₃O₂
• Molecular Weight: 281.314
• Mol file: 640732-63-4.mol

Synonyms:(4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile

Chemical Property of (4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile

There total 2 articles about (4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-aniline (104-94-9) → (4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile (640732-63-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanolic KOH-solution

2: basic lead carbonate; aqueous ethanol / 50 - 60 °C

With potassium hydroxide; ethanol; basic lead(II) carbonate;

Reference yield:

1,3-bis-(p-methoxyphenyl)thiourea (1227-45-8) → (4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile (640732-63-4)

Guidance literature:

Reference yield:

(4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile (640732-63-4) → 5-methoxyisatine (39755-95-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous ammonium polysulfide / 45 °C

2: concentrated sulfuric acid / und Erhitzen des Reaktionsgemisches mit Wasser

With ammonium polysulfide; sulfuric acid;

upstream raw materials:

1,3-bis-(p-methoxyphenyl)thiourea

4-methoxy-aniline

Downstream raw materials:

(4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide

5-methoxyisatine