N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide

Base Information

Chemical Name:N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide
CAS No.:141063-84-5
Molecular Formula:C₁₆H₂₁ClN₂O
Molecular Weight:292.809
Hs Code.:

Synonyms:N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide

Chemical Property:

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Technology Process of N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide

There total 4 articles about N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 141063-94-7
N-methyl-4-(dimethylamino)-1-methyl-2-butynylamine

: 41904-39-6
3-chloro-benzeneacetyl chloride

: 141063-84-5
N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide

Guidance literature:: With sodium hydroxide; In dichloromethane; water; for 2.5h; Ambient temperature;
DOI:10.1021/jm00093a011

Reference yield:

: 1878-65-5
3-chlorophenylacetic acid

: 141063-84-5
N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 1.) RT, 15 h, 2.) 70 deg C, 1 h

2: 94 percent / NaOH / CH₂Cl₂; H₂O / 2.5 h / Ambient temperature

With sodium hydroxide; thionyl chloride; In dichloromethane; water;
DOI:10.1021/jm00093a011

Reference yield:

: 111903-31-2
2,2,2-Trifluoro-N-methyl-N-(1-methyl-prop-2-ynyl)-acetamide

: 141063-84-5
N-methyl-N-<4-(dimethylamino)-1-methyl-2-butynyl>-2-(3-chlorophenyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / cuprous chloride, acetic acid / dioxane / 46 h / Ambient temperature

2: 80 percent / sodium borohydride / ethanol / 1 h / Ambient temperature

3: 94 percent / NaOH / CH₂Cl₂; H₂O / 2.5 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; acetic acid; copper(l) chloride; In 1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1021/jm00093a011