4-(1-acetyl-3-phenyl-4,5-dihydro-1H-pyrazol-5-yl)phenyl methyl ether

Base Information

Chemical Name:4-(1-acetyl-3-phenyl-4,5-dihydro-1H-pyrazol-5-yl)phenyl methyl ether
CAS No.:36988-80-4
Molecular Formula:C₁₈H₁₈N₂O₂
Molecular Weight:294.353
Hs Code.:
Mol file:36988-80-4.mol

Synonyms:1-acetyl-5-(4-methoxyphenyl)-3-phenyl-4,5-dihydro-(1H)-pyrazole

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Chemical Property of 4-(1-acetyl-3-phenyl-4,5-dihydro-1H-pyrazol-5-yl)phenyl methyl ether

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Technology Process of 4-(1-acetyl-3-phenyl-4,5-dihydro-1H-pyrazol-5-yl)phenyl methyl ether

There total 11 articles about 4-(1-acetyl-3-phenyl-4,5-dihydro-1H-pyrazol-5-yl)phenyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 64-19-7,77671-22-8
acetic acid

: 76973-46-1
5-(4-methoxyphenyl)-3-phenyl-4,5-dihydro-1H-pyrazole

: 36988-80-4
1-acetyl-5-(4-methoxyphenyl)-3-phenyl-4,5-dihydro-(1H)-pyrazole

Guidance literature:: at 110 ℃; for 1h; Temperature; Time; Solvent;
DOI:10.1080/00397911.2015.1104357

Reference yield: 88.67%

: 64-19-7,77671-22-8
acetic acid

: 959-33-1
3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one

: 36988-80-4
1-acetyl-5-(4-methoxyphenyl)-3-phenyl-4,5-dihydro-(1H)-pyrazole

Guidance literature:: With hydrazine hydrate; for 3h; Reflux;
DOI:10.1016/j.bmc.2014.05.037

Reference yield: 85.0%

: 22252-15-9
trans-4-methoxychalcone

: 64-19-7,77671-22-8
acetic acid

: 36988-80-4
1-acetyl-5-(4-methoxyphenyl)-3-phenyl-4,5-dihydro-(1H)-pyrazole

Guidance literature:: trans-4-methoxychalcone; acetic acid; With hydrogenchloride; In water; at 60 - 65 ℃; for 0.5h;

With hydrazine hydrate; In water; Reflux;