PH2P(SIME3)

Base Information

Chemical Name:PH2P(SIME3)
CAS No.:24103-44-4
Molecular Formula:C12H23 P Si2
Molecular Weight:254.459
Hs Code.:2931900090
Mol file:24103-44-4.mol

Synonyms:Bis(trimethylsilyl)phenylphosphine;Phenylbis(trimethylsilyl)phosphine

Suppliers and Price of PH2P(SIME3)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of PH2P(SIME3)

Chemical Property:

Boiling Point:103-105 °C(Press: 1.0 Torr)
PSA：13.59000
LogP:4.46360

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of PH2P(SIME3)

There total 5 articles about PH2P(SIME3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75-77-4
chloro-trimethyl-silane

: 638-21-1
phenylphosphane

: 24103-44-4
bis(trimethylsilyl)phenylphosphine

Guidance literature:: phenylphosphane; With methyllithium; In diethyl ether; at -10 - 20 ℃; for 4h; Glovebox; Reflux;

chloro-trimethyl-silane; In diethyl ether; at -78 - 20 ℃; for 10h; Glovebox;
DOI:10.1002/ejic.201801322

Reference yield: 77.0%

: 75-77-4
chloro-trimethyl-silane

: H₂PC₆H₅*O(C₂H₅)2

: 24103-44-4
bis(trimethylsilyl)phenylphosphine

Guidance literature:: H₂PC₆H₅*O(C₂H₅)2; With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃; for 2.3h; Inert atmosphere; Schlenk technique; Glovebox;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1039/d0dt00864h

Reference yield:

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 638-21-1
phenylphosphane

: 24103-44-4
bis(trimethylsilyl)phenylphosphine

Guidance literature:: trimethylsilyl trifluoromethanesulfonate; With triethylamine; In diethyl ether; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;

phenylphosphane; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/ja310680x