2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester

Base Information

Chemical Name:2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester
CAS No.:352322-18-0
Molecular Formula:C₂₆H₂₉ClN₂O₈
Molecular Weight:532.978
Hs Code.:

2,2-dimethyl-propionic acid [<i>N</i>'-benzoyl-<i>N</i>'-<i>tert</i>-butyl-<i>N</i>-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester

Synonyms:2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester

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Chemical Property of 2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester

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Technology Process of 2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester

There total 3 articles about 2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 352322-05-5
2-(benzoyloxy)-1-[(2,2-dimethylpropanoyl)oxy]-2-oxoethyl 2-benzoyl-2-tert-butyl-1-(4-chlorobenzoyl)hydrazinecarboxylate

: 352322-18-0
2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 1h; under 2844.31 Torr;
DOI:10.1055/s-2002-20036

Reference yield:

: 353757-96-7
2-(benzyloxy)-1-chloro-2-oxoethyl 2-benzoyl-2-tert-butyl-1-(4-chlorobenzoyl)hydrazinecarboxylate

: 352322-18-0
2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / NaI / acetone / 2 h / 30 °C

2: 80 percent / DIEA / tetrahydrofuran / 16 h / 20 °C

3: 100 percent / H₂ / 10 percent Pd/C / ethyl acetate / 1 h / 2844.31 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate; acetone; 1: Finkelstein reaction;
DOI:10.1055/s-2002-20036

Reference yield:

: 352321-51-8
[N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-iodo-acetic acid benzyl ester

: 352322-18-0
2,2-dimethyl-propionic acid [N'-benzoyl-N'-tert-butyl-N-(4-chloro-benzoyl)-hydrazinocarbonyloxy]-carboxy-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DIEA / tetrahydrofuran / 16 h / 20 °C

2: 100 percent / H₂ / 10 percent Pd/C / ethyl acetate / 1 h / 2844.31 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1055/s-2002-20036