1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate

Base Information

Chemical Name:1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate
CAS No.:129363-77-5
Molecular Formula:C₂₀H₂₇NO₄S
Molecular Weight:377.505
Hs Code.:

Synonyms:1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate

Suppliers and Price of 1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate

There total 2 articles about 1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 63006-68-8
tert-butyl (phenylthio)acetate

: N-<3-(dimethylamino)-3-(ethoxycarbonyl)-2-propenylidene>-N-methylmethanaminium tetrafluoroborate

: 129363-77-5
1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate

Guidance literature:: With n-butyllithium; In ethanol; for 2.33333h; Ambient temperature;
DOI:10.1021/jm00172a010

Reference yield:

: 67751-14-8
ethyl 4-(dimethylamino)-2-oxo-3-butenoate

: 129363-77-5
1-ethyl 6-tert-butyl 2-(dimethylamino)-5-(phenylthio)-2,4-hexadienedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triethyloxonium tetrafluoroborate / 1.) CH₂Cl₂, RT, 5 h, 2.) Et₂O, 5 deg C, 15 h

2: 61 percent / n-BuLi / ethanol / 2.33 h / Ambient temperature

With n-butyllithium; triethyloxonium fluoroborate; In ethanol;
DOI:10.1021/jm00172a010