2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester

Base Information

• Chemical Name: 2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester
• CAS No.: 698358-23-5
• Molecular Formula: C₂₃H₂₈N₂O₂
• Molecular Weight: 364.488

Synonyms:2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester

Chemical Property of 2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester

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Technology Process of 2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester

There total 3 articles about 2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine (93102-05-7) + propynoic acid ethyl ester (623-47-2) → 2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester (698358-23-5)

Guidance literature:

With trifluoroacetic acid; In tetrahydrofuran; at 0 - 20 ℃; for 10.5h;

Reference yield: 86.0%

N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine (93102-05-7) + propynoic acid ethyl ester (623-47-2) → ethyl 1-benzyl-2,5-dihydro-1H-pyrrole-3-carboxylate (128259-46-1) + 2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester (698358-23-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1016/j.tetlet.2004.02.114

Reference yield:

N-ethyl-N-<(trimethylsilyl)methyl>benzylamine (111267-97-1) + propynoic acid ethyl ester (623-47-2) → 2,5-Dibenzyl-hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester (698358-23-5)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 10h; Reagent/catalyst; Reflux;

upstream raw materials:

N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine

propynoic acid ethyl ester

N-ethyl-N-<(trimethylsilyl)methyl>benzylamine

Downstream raw materials:

2-tert-Butyl 3a-Ethyl Tetrahydropyrrolo[3,4-c]pyrrole-2,3a(1H,3H)-dicarboxylate

Hexahydro-pyrrolo[3,4-c]pyrrole-3a-carboxylic Acid Ethyl Ester

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