1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene

Base Information

Chemical Name:1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene
CAS No.:1352922-02-1
Molecular Formula:C₁₇H₁₉F₃
Molecular Weight:280.333
Hs Code.:

Synonyms:1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene

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Technology Process of 1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene

There total 8 articles about 1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 205108-18-5
(E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

: 1352922-02-1
1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene

Guidance literature:: With CoBr₂(SchmalzPhos); zinc(II) iodide; zinc; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201103613

Reference yield:

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 205108-18-5
(E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

: 1352922-02-1
1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene

: 1352922-17-8
1-trifluoromethyl-4-((E)-5,6-dimethyl-3-methylenehepta-1,5-dienyl)benzene

Guidance literature:: With cobalt(II) bromide-[1,2-bis(diphenylphosphino)ethane]; zinc(II) iodide; zinc; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201103613

Reference yield:

: 402-43-7
p-trifluoromethylphenyl bromide

: 1352922-02-1
1-[(1E,3E)-6,7-dimethylocta-1,3,6-trien-1-yl]-4-(trifluoromethyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: potassium chloride; tetrabutylammonium acetate; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 90 °C

2: hydrogenchloride / water

3: potassium tert-butylate / diethyl ether / 1 h / 0 - 20 °C / Inert atmosphere

4: CoBr₂(SchmalzPhos); zinc(II) iodide; zinc / dichloromethane / 20 °C / Inert atmosphere

With hydrogenchloride; CoBr₂(SchmalzPhos); potassium chloride; potassium tert-butylate; tetrabutylammonium acetate; palladium diacetate; potassium carbonate; zinc(II) iodide; zinc; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 1: Heck type coupling / 3: Wittig reaction;
DOI:10.1002/anie.201103613