(E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

Base Information

Chemical Name:(E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene
CAS No.:205108-18-5
Molecular Formula:C₁₁H₉F₃
Molecular Weight:198.188
Hs Code.:

Synonyms:(E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

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Technology Process of (E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

There total 13 articles about (E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 95123-61-8
(2E)-3-(4-trifluoromethylphenyl)prop-2-enal

: 205108-18-5
(E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.333333h; Inert atmosphere;

(2E)-3-(4-trifluoromethylphenyl)prop-2-enal; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere;
DOI:10.1039/d0cc02697b

Reference yield: 75.0%

: 77-79-2
3-Sulfolene

: 402-43-7
p-trifluoromethylphenyl bromide

: 205108-18-5
(E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

Guidance literature:: 3-Sulfolene; With o-phenylenebis(diphenylphosphine); potassium methanolate; palladium diacetate; potassium carbonate; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Sealed tube; Inert atmosphere;

p-trifluoromethylphenyl bromide; In tetrahydrofuran; at 20 - 110 ℃; for 13.3333h; stereoselective reaction; Sealed tube;
DOI:10.1021/jacs.8b05421

Reference yield: 70.0%

: 77-79-2
3-Sulfolene

: 146397-87-7
p-(trifluoromethyl)phenyl trifluoromethanesulfonate

: 205108-18-5
(E)-1-(buta-1,3-dien-1-yl)-4-(trifluoromethyl)benzene

Guidance literature:: 3-Sulfolene; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h;

With o-phenylenebis(diphenylphosphine); palladium diacetate; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;

p-(trifluoromethyl)phenyl trifluoromethanesulfonate; With potassium hydrogencarbonate; In tetrahydrofuran; at 20 - 100 ℃; stereoselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1016/j.tet.2019.04.012