1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
CAS No.:1000870-47-2
Molecular Formula:C₃₁H₄₀BF₂N₃O₄
Molecular Weight:567.484
Hs Code.:

Synonyms:1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 2 articles about 1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 120-21-8
4-Diethylaminobenzaldehyde

: 54474-51-0
methyl 2,4-dimethyl-3-pyrrolepropionate

: 1000870-47-2
1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: 4-Diethylaminobenzaldehyde; methyl 2,4-dimethyl-3-pyrrolepropionate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

With boron trifluoride diethyl etherate; triethylamine; In 1,2-dichloro-ethane; for 0.666667h; Reflux; Inert atmosphere;
DOI:10.1039/c1cc12947c

Reference yield:

: C₃₁H₄₃N₃O₄

: 1000870-47-2
1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In toluene; at 20 ℃; for 0.166667h;

Reference yield: 91.0%

: 1000870-47-2
1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

: 1000870-48-3
bis-carboxylic acid (1,3,5,7-tetramethyl-2,6-bis(2-carboxyethyl)-8-(p-diethylaminophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene)

Guidance literature:: 1,3,5,7-tetramethyl-2,6-bis(2-methoxycarbonylethyl)-8-[4-(N,N-diethylamino)phenyl]-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene; With sodium hydroxide; water; In methanol; dichloromethane; acetone; at 20 ℃; for 4h;

With hydrogenchloride; In methanol; dichloromethane; water; UV-irradiation;