N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide

Base Information

Chemical Name:N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide
CAS No.:132451-14-0
Molecular Formula:C₂₁H₁₉N₃O₅S₂
Molecular Weight:457.531
Hs Code.:

Synonyms:N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide

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Chemical Property of N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide

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Technology Process of N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide

There total 4 articles about N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132451-28-6
1-(5-methyl-2-phenyl-1,3-oxazol-4-yl)methanamine

: 125758-75-0
4-<(2,4-dioxothiazolidin-5-yl)methyl>benzenesulfonyl chloride

: 132451-14-0
N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm00088a022

Reference yield:

: 3774-99-0
5-benzylidene-2,4-thiazolidinedione

: 132451-14-0
N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / H₂ / 10 percent Pd/C / tetrahydrofuran; acetic acid

2: chlorosulfonic acid / 0.5 h / Ambient temperature

3: i-Pr₂EtN / CH₂Cl₂

With chlorosulfonic acid; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1021/jm00088a022

Reference yield:

: 33321-31-2
5-(Benzyl)thiazolidine-2,4-dione

: 132451-14-0
N-[(5-Methyl-2-phenyl-4-oxazolyl)methyl]-4-[(thiazolidine-2,4-dion-5-yl)methyl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / 0.5 h / Ambient temperature

2: i-Pr₂EtN / CH₂Cl₂

With chlorosulfonic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm00088a022