2-FLUORO-2-METHANESULFONYLOXYMETHYL-MALONIC ACID DIETHYL ESTER

Base Information

• Chemical Name: 2-FLUORO-2-METHANESULFONYLOXYMETHYL-MALONIC ACID DIETHYL ESTER
• CAS No.: 2710-86-3
• Molecular Formula: C9H15 F O7 S
• Molecular Weight: 286.278
• Hs Code.: 2918990090
• Mol file: 2710-86-3.mol

Synonyms:Malonicacid, fluoro(hydroxymethyl)-, diethyl ester, methanesulfonate (7CI,8CI)

Chemical Property of 2-FLUORO-2-METHANESULFONYLOXYMETHYL-MALONIC ACID DIETHYL ESTER

Chemical Property:

• Boiling Point: 145-7°C 0,08mm
• PSA: 104.35000
• Density: 1.319±0.06 g/cm3(Predicted)
• LogP: 0.87790

Purity/Quality:

99% ^*data from raw suppliers

Diethyl2-fluoro-2-(((methylsulfonyl)oxy)methyl)malonate 97% ^*data from reagent suppliers

Safty Information:

• Statements: 34-36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-FLUORO-2-METHANESULFONYLOXYMETHYL-MALONIC ACID DIETHYL ESTER

There total 1 articles about 2-FLUORO-2-METHANESULFONYLOXYMETHYL-MALONIC ACID DIETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl 2-fluoro-2-(hydroxymethyl)malonate (756-31-0) + methanesulfonyl chloride (124-63-0) → Diaethyl-α-fluor-α-methansulfonyloxymethyl-malonat (2710-86-3)

Guidance literature:

With pyridine; In benzene;

DOI:10.1039/jr9610004669

Reference yield: 77.8%

Diaethyl-α-fluor-α-methansulfonyloxymethyl-malonat (2710-86-3) → ethyl 2-fluoroacrylate (760-80-5)

Guidance literature:

With 2,6-di-tert-butyl-4-methyl-phenol; In dimethyl sulfoxide; at 160 ℃; for 11h;

upstream raw materials:

diethyl 2-fluoro-2-(hydroxymethyl)malonate

methanesulfonyl chloride

Downstream raw materials:

ethyl 2-fluoroacrylate

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