S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide

Base Information

Chemical Name:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide
CAS No.:1147095-83-7
Molecular Formula:C₂₄H₂₃Cl₂N₅O₄S
Molecular Weight:548.45
Hs Code.:

Synonyms:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide

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Chemical Property of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide

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Technology Process of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide

There total 12 articles about S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1147095-62-2,1147096-65-8
5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)benzamide

: 124-40-3
dimethyl amine

: 1147095-83-7
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 25 - 30 ℃; for 12h;
DOI:10.1016/j.ejmech.2012.10.005

Reference yield:

: 280771-82-6
N-(5-chloropyridin-2-yl)-5-chloro-2-nitrobenzamide

: 1147095-83-7
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide

Guidance literature:: Multi-step reaction with 5 steps

1: tin(II) chloride dihdyrate / ethyl acetate / 2 h / 25 - 30 °C

2: tetrahydrofuran / 12 h / 10 - 30 °C / Inert atmosphere

3: sulfuric acid / 0 - 5 °C

4: pyridine / dichloromethane / 0 °C

5: potassium iodide / N,N-dimethyl-formamide; water / 12 h / 25 - 30 °C

With pyridine; tin(II) chloride dihdyrate; sulfuric acid; potassium iodide; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 229343-30-0
2-amino-5-chloro-N-(5-chloro-pyridin-2-yl)-benzamide

: 1147095-83-7
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-(2-dimethylamino-acetyl)sulfoximide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 12 h / 10 - 30 °C / Inert atmosphere

2: sulfuric acid / 0 - 5 °C

3: pyridine / dichloromethane / 0 °C

4: potassium iodide / N,N-dimethyl-formamide; water / 12 h / 25 - 30 °C

With pyridine; sulfuric acid; potassium iodide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;