2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Base Information

Chemical Name:2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile
CAS No.:1267605-19-5
Molecular Formula:C₄₀H₃₇F₃N₄O₂S
Molecular Weight:694.821
Hs Code.:

2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Synonyms:2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Suppliers and Price of 2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

There total 5 articles about 2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.5%

: 1267605-15-1
3-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]propenal

: 436097-14-2
[3-cyano-4-methyl-5-phenyl-5-(trifluoromethyl)-2(5H)-furanylidene]propanedinitrile

: 1267605-19-5
2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Guidance literature:: In tetrahydrofuran; ethanol; at 50 ℃; for 4h;

Reference yield:

: N,N-dibutyl-4-amino-2-hydroxy-benzaldehyde

: 1267605-19-5
2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 2 h / 50 °C

2.1: phenyllithium / dibutyl ether; tetrahydrofuran / 1.5 h / Cooling with ice; Inert atmosphere

3.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -73 - -70 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran / 0.5 h / Cooling with ice

4.2: 1 h

5.1: diisobutylaluminium hydride / toluene / 1.25 h / -76 - -75 °C / Inert atmosphere

5.2: 0.5 h

6.1: ethanol; tetrahydrofuran / 4 h / 50 °C

With n-butyllithium; sodium hydride; diisobutylaluminium hydride; potassium carbonate; phenyllithium; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; hexane; dibutyl ether; toluene;

Reference yield:

: 103893-16-9
4-N,N-di-n-butylamino-2-methoxybenzaldehyde

: 1267605-19-5
2-[4-[4-[5-[2-(4-dibutylamino-2-methoxyphenyl)vinyl]thiophene-2-yl]-1,3-butadienyl]-3-cyano-5-phenyl-5-trifluoromethyl-2(5H)-furanylidene]propanedinitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: phenyllithium / dibutyl ether; tetrahydrofuran / 1.5 h / Cooling with ice; Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -73 - -70 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran / 0.5 h / Cooling with ice

3.2: 1 h

4.1: diisobutylaluminium hydride / toluene / 1.25 h / -76 - -75 °C / Inert atmosphere

4.2: 0.5 h

5.1: ethanol; tetrahydrofuran / 4 h / 50 °C

With n-butyllithium; sodium hydride; diisobutylaluminium hydride; phenyllithium; In tetrahydrofuran; ethanol; hexane; dibutyl ether; toluene;