POLY(2-PHENYLETHYL METHACRYLATE)

Base Information

• Chemical Name: POLY(2-PHENYLETHYL METHACRYLATE)
• CAS No.: 28825-60-7
• Molecular Formula: C12H14O2
• Molecular Weight: 190.24
• Mol file: 28825-60-7.mol

Synonyms:POLY(2-PHENYLETHYL METHACRYLATE)

Chemical Property of POLY(2-PHENYLETHYL METHACRYLATE)

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of POLY(2-PHENYLETHYL METHACRYLATE)

There total 5 articles about POLY(2-PHENYLETHYL METHACRYLATE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

2-phenylethanol (60-12-8) + Methacryloyl chloride (920-46-7,26937-45-1) → 2-phenylethyl methacrylate (3683-12-3,28825-60-7)

Guidance literature:

2-phenylethanol; With triethylamine; In dichloromethane; for 0.0833333h; Cooling with ice;

Methacryloyl chloride; In dichloromethane; at 0 - 20 ℃;

DOI:10.1111/php.12038

Reference yield:

2-phenylethanol (60-12-8) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → 2-phenylethyl methacrylate (3683-12-3,28825-60-7)

Guidance literature:

With sulfuric acid; hydroquinone; benzene; at 130 - 136 ℃; Erhitzen unter Abdestillieren des entstehenden Methanols;

Reference yield:

poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) + 2-phenylethanol (60-12-8) → 2-phenylethyl methacrylate (3683-12-3,28825-60-7)

Guidance literature:

With toluene-4-sulfonic acid; hydroquinone; In benzene; for 9h; Yield given; Heating;

upstream raw materials:

2-phenylethyl 2-hydroxy-2-methylpropionate

2-phenylethanol

methacrylic acid methyl ester

poly(methacrylic acid)

Refernces

• 1、 Tokuyasu, Takahiro,Kunikawa, Shigeki,McCullough, Kevin J.,Masuyama, Araki,Nojima, Masatomo. "Synthesis of cyclic peroxides by chemo- and regioselective peroxidation of dienes with Co(II)/O2/Et3SiH". . p. 251 - 260. Retrieved 2007/10/03.