(2R,3S)-2-azido-3-phenylisohexanoic acid

Base Information

Chemical Name:(2R,3S)-2-azido-3-phenylisohexanoic acid
CAS No.:199468-83-2
Molecular Formula:C₁₂H₁₅N₃O₂
Molecular Weight:233.27
Hs Code.:

Synonyms:(2R,3S)-2-azido-3-phenylisohexanoic acid

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Chemical Property of (2R,3S)-2-azido-3-phenylisohexanoic acid

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Technology Process of (2R,3S)-2-azido-3-phenylisohexanoic acid

There total 10 articles about (2R,3S)-2-azido-3-phenylisohexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 199468-80-9
(S)-3-((2R,3S)-2-Azido-4-methyl-3-phenyl-pentanoyl)-4-phenyl-oxazolidin-2-one

: 199468-83-2
(2R,3S)-2-azido-3-phenylisohexanoic acid

Guidance literature:: With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; for 3h;
DOI:10.1016/S0040-4020(97)10127-2

Reference yield:

: 176018-91-0
(S)-3-((S)-4-Methyl-3-phenyl-pentanoyl)-4-phenyl-oxazolidin-2-one

: 199468-83-2
(2R,3S)-2-azido-3-phenylisohexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) diisopropylethylamine, dibutylboron triflate, 2.) N-bromosuccinimide / 1.) CH₂Cl₂, 2.) CH₂Cl₂

2: 78 percent / tetramethylguanidine azide / acetonitrile / 24 h / Ambient temperature

3: 70 percent / hydrogen peroxide, lithium hydroxide monohydrate / tetrahydrofuran; H₂O / 3 h

With lithium hydroxide; N-Bromosuccinimide; di-n-butylboryl trifluoromethanesulfonate; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; tetramethylguanidinum azide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1016/S0040-4020(97)10127-2

Reference yield:

: 199468-77-4
(S)-3-((2S,3S)-2-Bromo-4-methyl-3-phenyl-pentanoyl)-4-phenyl-oxazolidin-2-one

: 199468-83-2
(2R,3S)-2-azido-3-phenylisohexanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / tetramethylguanidine azide / acetonitrile / 24 h / Ambient temperature

2: 70 percent / hydrogen peroxide, lithium hydroxide monohydrate / tetrahydrofuran; H₂O / 3 h

With lithium hydroxide; dihydrogen peroxide; tetramethylguanidinum azide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1016/S0040-4020(97)10127-2