4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate

Base Information

Chemical Name:4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate
CAS No.:143887-97-2
Molecular Formula:C₇H₅ClO₂*C₁₄H₁₉NO
Molecular Weight:373.879
Hs Code.:

Synonyms:4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate

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Technology Process of 4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate

There total 2 articles about 4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 90986-85-9
PPTP

: 937-14-4
3-chloro-benzenecarboperoxoic acid

: 143887-97-2
4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate

Guidance literature:: In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/jm00100a023

Reference yield:

: 27132-46-3
1-propyl-4-phenylpyridinium iodide

: 143887-97-2
4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 1 h / 0 °C

2: 64 percent / CH₂Cl₂ / 2 h / 0 °C

With sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1021/jm00100a023

Reference yield: 45.0%

: 143887-97-2
4-phenyl-1-propyl-1,2,3,6-tetrahydropyridine N-oxide m-chlorobenzoate

: 4-phenyl-1-propyl-2,3-dihydropyridinium perchlorate

Guidance literature:: With aluminum oxide; perchloric acid; trifluoroacetic anhydride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jm00100a023