N-Ethyl-3,5-dimethylaniline

Base Information

• Chemical Name: N-Ethyl-3,5-dimethylaniline
• CAS No.: 13342-22-8
• Molecular Formula: C₁₀H₁₅N
• Molecular Weight: 149.236
• Mol file: 13342-22-8.mol

Synonyms:3,5-dimethyl-N-ethylaniline

Chemical Property of N-Ethyl-3,5-dimethylaniline

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

N-Ethyl-3,5-dimethylaniline ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Ethyl-3,5-dimethylaniline

There total 3 articles about N-Ethyl-3,5-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

acetic acid (64-19-7,77671-22-8) + 3,5-dimethylaminoaniline (108-69-0) → 3,5-dimethyl-N-ethylaniline (13342-22-8)

Guidance literature:

With cobalt(II) tetrafluoroborate hexahydrate; hydrogen; bis(2-diphenylphosphinoethyl)phenylphosphine; In dibutyl ether; at 120 ℃; for 24h; under 45004.5 Torr; Green chemistry;

DOI:10.1002/cssc.201802144

Reference yield:

ethyl bromide (74-96-4) + 3,5-dimethylaminoaniline (108-69-0) → 3,5-dimethyl-N-ethylaniline (13342-22-8)

Guidance literature:

With potassium carbonate; potassium iodide; In tetrahydrofuran; at 40 ℃; for 6h; Inert atmosphere;

DOI:10.1021/la2027253

Reference yield:

→ 3,5-dimethyl-N-ethylaniline (13342-22-8)

Guidance literature:

2,4,6-Trimethyl-pyryliumperchlorat, Aethylamin ( 2 Mol), H2O, Δ; (geringe Ausb.; Nebenprod.: 1-Aethyl-2,4,6-trimethyl-pyridinium-perchlorat);

upstream raw materials:

ethyl bromide

3,5-dimethylaminoaniline

acetic acid

Downstream raw materials:

C₄₂H₆₀N₆O₆

2-(3,5-dimethylphenyl)-1,2,3,4-tetrahydroisoquinoline

N (dimethyl-3,5-phenyl-1) pyrrolidine

C₂₂H₂₀FNO₂S

Refernces

• 1、 Wang, Xiaolin,Yin, Jianjun,Wang, Xiaogong. "Photoinduced self-structured surface pattern on a molecular azo glass film: Structure-property relationship and wavelength correlation". experimental part. p. 12666 - 12676. Retrieved 2012/06/18.