(-)-(1S)-bis-m-xylylenediamine

Base Information

Chemical Name:(-)-(1S)-bis-m-xylylenediamine
CAS No.:155906-89-1
Molecular Formula:C₂₆H₄₄N₂O₄
Molecular Weight:448.646
Hs Code.:

(-)-(1S)-bis<N-ethyl-N-(1-isobutyl-1-ethoxycarbonyl)-methyl>-m-xylylenediamine

Synonyms:(-)-(1S)-bis-m-xylylenediamine

Suppliers and Price of (-)-(1S)-bis-m-xylylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1S)-bis-m-xylylenediamine

Chemical Property:

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Technology Process of (-)-(1S)-bis-m-xylylenediamine

There total 4 articles about (-)-(1S)-bis-m-xylylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 75-03-6
ethyl iodide

: 155906-92-6
(-)-(1S)-bis-m-xylylenediamine

: 155906-89-1
(-)-(1S)-bis-m-xylylenediamine

Guidance literature:: With sodium carbonate; In acetonitrile; for 48h; Heating;
DOI:10.1016/S0957-4166(00)80484-X

Reference yield:

: 626-19-7
Isophthalaldehyde

: 155906-89-1
(-)-(1S)-bis-m-xylylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: molecular sieves / CH₂Cl₂ / 2 h / Ambient temperature

2: NaBH₄ / methanol / 2 h / Ambient temperature

3: 92 percent / Na₂CO₃ / acetonitrile / 48 h / Heating

With sodium tetrahydroborate; molecular sieve; sodium carbonate; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0957-4166(00)80484-X

Reference yield:

: 2666-93-5
(S)-Leu-OMe

: 155906-89-1
(-)-(1S)-bis-m-xylylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: molecular sieves / CH₂Cl₂ / 2 h / Ambient temperature

2: NaBH₄ / methanol / 2 h / Ambient temperature

3: 92 percent / Na₂CO₃ / acetonitrile / 48 h / Heating

With sodium tetrahydroborate; molecular sieve; sodium carbonate; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0957-4166(00)80484-X