ethyl 2-(diphenyl methylene amino)-3-(4-isopropylphenyl) propanoate

Base Information

Chemical Name:ethyl 2-(diphenyl methylene amino)-3-(4-isopropylphenyl) propanoate
CAS No.:1354521-86-0
Molecular Formula:C₂₇H₂₉NO₂
Molecular Weight:399.533
Hs Code.:

Synonyms:ethyl 2-(diphenyl methylene amino)-3-(4-isopropylphenyl) propanoate

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Chemical Property of ethyl 2-(diphenyl methylene amino)-3-(4-isopropylphenyl) propanoate

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Technology Process of ethyl 2-(diphenyl methylene amino)-3-(4-isopropylphenyl) propanoate

There total 2 articles about ethyl 2-(diphenyl methylene amino)-3-(4-isopropylphenyl) propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 69555-14-2
ethyl N-diphenylmethylene glycine

: 73789-86-3
4-i-propylbenzyl bromide

: 1354521-86-0
ethyl 2-(diphenyl methylene amino)-3-(4-isopropylphenyl) propanoate

Guidance literature:: ethyl N-diphenylmethylene glycine; With potassium hydroxide; In dimethyl sulfoxide; at 0 ℃; for 0.0833333h; Inert atmosphere;

4-i-propylbenzyl bromide; In dimethyl sulfoxide; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol2031747

Reference yield:

: 119-61-9
benzophenone

: 1354521-86-0
ethyl 2-(diphenyl methylene amino)-3-(4-isopropylphenyl) propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 0.5 h / Inert atmosphere; Reflux

1.2: 3 h / Inert atmosphere; Reflux

2.1: potassium hydroxide / dimethyl sulfoxide / 0.08 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 - 20 °C / Inert atmosphere

With potassium hydroxide; In dimethyl sulfoxide; toluene;
DOI:10.1021/ol2031747