(5,6-dichloro-3-methylsulfanyl-pyrazin-2-yl)-(4-fluoro-phenyl)-methanone

Base Information

Chemical Name:(5,6-dichloro-3-methylsulfanyl-pyrazin-2-yl)-(4-fluoro-phenyl)-methanone
CAS No.:1174517-60-2
Molecular Formula:C₁₂H₇Cl₂FN₂OS
Molecular Weight:317.171
Hs Code.:

Synonyms:(5,6-dichloro-3-methylsulfanyl-pyrazin-2-yl)-(4-fluoro-phenyl)-methanone

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Chemical Property of (5,6-dichloro-3-methylsulfanyl-pyrazin-2-yl)-(4-fluoro-phenyl)-methanone

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Technology Process of (5,6-dichloro-3-methylsulfanyl-pyrazin-2-yl)-(4-fluoro-phenyl)-methanone

There total 1 articles about (5,6-dichloro-3-methylsulfanyl-pyrazin-2-yl)-(4-fluoro-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1174517-48-6
2,3-dichloro-5-methylsulfanyl-pyrazine

: TMPMgCl*LiCl

: C₅H₃Cl₄LiMgN₂S

: 403-43-0
4-fluorobenzoyl chloride

: 1174517-60-2
(5,6-dichloro-3-methylsulfanyl-pyrazin-2-yl)-(4-fluoro-phenyl)-methanone

Guidance literature:: 2,3-dichloro-5-methylsulfanyl-pyrazine; TMPMgCl*LiCl; With zinc(II) chloride; In tetrahydrofuran; at -40 ℃; for 1h; Inert atmosphere;

C₅H₃Cl₄LiMgN₂S; 4-fluorobenzoyl chloride; With copper(I) cyanide lithium chloride; In tetrahydrofuran; at -40 - -10 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/ol901275n