S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate

Base Information

• Chemical Name: S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate
• CAS No.: 783288-19-7
• Molecular Formula: C₂₁H₃₀Cl₂N₂O₂S
• Molecular Weight: 445.453

Synonyms:S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate

Chemical Property of S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate

Chemical Property:

Purity/Quality:

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Technology Process of S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate

There total 3 articles about S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitro-4,5-dichlorophenol (39224-65-2) → S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate (783288-19-7)

Guidance literature:

Multi-step reaction with 4 steps

1: NaH / dimethylformamide

2: diphenyl ether / 120 - 200 °C

3: SnCl₂*2H₂O / ethyl acetate

4: pyridine

With pyridine; sodium hydride; tin(ll) chloride; In diphenylether; ethyl acetate; N,N-dimethyl-formamide; 2: Newman-Kwart rearrangement;

DOI:10.1016/j.bmcl.2004.02.071

Reference yield:

→ S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate (783288-19-7)

Guidance literature:

Reference yield:

1-(3-methylbutyl)cyclohexanecarbonyl chloride + dimethyl-thiocarbamic acid S-(2-amino-4,5-dichloro-phenyl) ester → S-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl]N,N-dimethylthiocarbamate (783288-19-7)

Guidance literature:

With pyridine;

DOI:10.1016/j.bmcl.2004.02.071

upstream raw materials:

2-nitro-4,5-dichlorophenol

Downstream raw materials:

bis-[4,5-dichloro-2-(1-isopentylcyclohexanecarbonylamino)phenyl] disulfide

N-(4,5-dichloro-2-mercaptophenyl)-1-isopentylcyclohexanecarboxamide

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