(2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan

Base Information

Chemical Name:(2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan
CAS No.:183945-01-9
Molecular Formula:C₂₃H₂₆Cl₄O₆
Molecular Weight:540.268
Hs Code.:

Synonyms:(2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan

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Chemical Property of (2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan

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Technology Process of (2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan

There total 1 articles about (2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 627-42-9
2-chloroethyl methyl ether

: 168427-35-8
(3R,4S,5R)-4-((2,4-dichlorobenzyl)oxy)-5-(((2,4-dichlorobenzyl)oxy)methyl)-2-methoxytetrahydrofuran-3-ol

: 183945-01-9
(2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; for 28h; Ambient temperature;
DOI:10.1002/hlca.19960790716

Reference yield:

: 183945-01-9
(2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan

: 2'-O-(2-Methoxyethyl)-5-methyl-3',5'-bis-O-(4-toluoyl)thymidin

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / MgO, H₂ / 5percent Pd/C / methanol / 2 h / 35 °C

2: 96 percent / pyridine / 4 h / 20 °C

3: 83 percent / conc. H₂SO₄ / acetic acid / 18 h

4: 97 percent / SnCl₂ / acetonitrile / 8 h / 50 °C

With pyridine; sulfuric acid; hydrogen; magnesium oxide; tin(ll) chloride; palladium on activated charcoal; In methanol; acetic acid; acetonitrile;
DOI:10.1002/hlca.19960790716

Reference yield:

: 183945-01-9
(2R,3R,4R,5S)-3-(2,4-Dichloro-benzyloxy)-2-(2,4-dichloro-benzyloxymethyl)-5-methoxy-4-(2-methoxy-ethoxy)-tetrahydro-furan

: C₃₅H₃₄O₈

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / MgO, H₂ / 5percent Pd/C / methanol / 2 h / 35 °C

2: 93 percent / pyridine / 4 h / 20 °C

With pyridine; hydrogen; magnesium oxide; palladium on activated charcoal; In methanol;
DOI:10.1002/hlca.19960790716