N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate

Base Information

Chemical Name:N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate
CAS No.:943019-61-2
Molecular Formula:C₂₂H₃₄BNO₅
Molecular Weight:403.327
Hs Code.:

Synonyms:N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate

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Chemical Property of N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate

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Technology Process of N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate

There total 1 articles about N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 894793-37-4
benzyl N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate

: 943019-61-2
N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate

Guidance literature:: With hydrogen; 4.9 % palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 4h;

Reference yield: 77.0%

: 943019-61-2
N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate

: 143945-72-6
N-trityl-5-(2-bromophenyl)tetrazole

: 137862-53-4,137862-87-4
N-pentanoyl-N-[[2'-(1H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl]-methyl]-(L)-valine

Guidance literature:: N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate; N-trityl-5-(2-bromophenyl)tetrazole; With potassium phosphate; palladium diacetate; triphenylphosphine; In tetrahydrofuran; at 60 ℃;

With methanol; for 3h; Product distribution / selectivity; Heating / reflux;

Reference yield: 63.0%

: 943019-61-2
N-[4-(5,5-dimethyl-[1,3,2]dioxaborinan-2-yl)phenyl-4-yl-methyl]-N-pentanoyl-L-valinate

: 143945-72-6
N-trityl-5-(2-bromophenyl)tetrazole

: potassium N-pentanoyl-N-[{2'-(1-(triphenylmethyl)-1H-tetrazol-5-yl)-1,1'-biphenyl-4-yl}methyl]-L-valinate

Guidance literature:: With potassium phosphate; tetrabutylammomium bromide; palladium diacetate; triphenylphosphine; In tetrahydrofuran; toluene; at 80 ℃; Product distribution / selectivity;