5-amino-N₁-(1,3-dihydroxypropan-2-yl)-N₃-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

Base Information

• Chemical Name: 5-amino-N₁-(1,3-dihydroxypropan-2-yl)-N₃-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide
• CAS No.: 1096689-22-3
• Molecular Formula: C₁₄H₁₈I₃N₃O₆
• Molecular Weight: 705.027

Synonyms:5-amino-N₁-(1,3-dihydroxypropan-2-yl)-N₃-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

Chemical Property of 5-amino-N₁-(1,3-dihydroxypropan-2-yl)-N₃-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

Chemical Property:

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Technology Process of 5-amino-N₁-(1,3-dihydroxypropan-2-yl)-N₃-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

There total 2 articles about 5-amino-N₁-(1,3-dihydroxypropan-2-yl)-N₃-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

3-Amino-1,2-propanediol (616-30-8,13552-31-3,98923-21-8) + serinol (534-03-2) + 5-amino-2,4,6-triiodoisophthalic acid dichloride (37441-29-5) → 5-amino-N1-(1,3-dihydroxypropan-2-yl)-N3-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (1096689-22-3)

Guidance literature:

3-Amino-1,2-propanediol; 5-amino-2,4,6-triiodoisophthalic acid dichloride; With triethylamine; In N,N-dimethyl acetamide; at -24 - 2 ℃; for 24h;

serinol; In N,N-dimethyl acetamide; at 0 - 40 ℃; for 44h;

Reference yield: 56.0%

C14H21N3O6 → 5-amino-N1-(1,3-dihydroxypropan-2-yl)-N3-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (1096689-22-3)

Guidance literature:

With iodine; In methanol; at 60 - 65 ℃; for 4h; Reagent/catalyst; Temperature;

Reference yield: 100.0%

5-amino-N1-(1,3-dihydroxypropan-2-yl)-N3-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (1096689-22-3) + acetic anhydride (108-24-7) + acetic acid (64-19-7,77671-22-8) → Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester (1186058-05-8)

Guidance literature:

With NC₁₀₀₁₈₁; acetyl chloride; at 23 - 100 ℃; for 18h;

upstream raw materials:

3-Amino-1,2-propanediol

serinol

5-amino-2,4,6-triiodoisophthalic acid dichloride

Downstream raw materials:

Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester

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