benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside

Base Information

Chemical Name:benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside
CAS No.:129162-96-5
Molecular Formula:C₆₃H₆₇NO₁₂
Molecular Weight:1030.22
Hs Code.:

Synonyms:benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside

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Chemical Property of benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside

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Technology Process of benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside

There total 8 articles about benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62447-55-6
Benzyl 2,4,6-tri-O-benzyl-β-D-galactopyranoside

: 129162-96-5
benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / AW-300 molecular sieves, BF₃*Et₂O / 1,2-dichloro-ethane / 2 h / -30 °C

2: NH₂NH₂*H₂O / ethanol / 2 h / Heating

3: pyridine / 1 h / 20 °C

With pyridine; molecular sieve; boron trifluoride diethyl etherate; hydrazine hydrate; In ethanol; 1,2-dichloro-ethane;
DOI:10.1016/0008-6215(90)84224-I

Reference yield:

: 100-39-0
benzyl bromide

: 129162-96-5
benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / Ag₂O, KI / dimethylformamide / 4 h / 0 - 20 °C

2: 1.) tris(triphenylphosphine)rhodium(I) chloride, 1,4-diazabicyclo<2.2.2>octane 2.) HgO, HgCl₂ / 1a) EtOH, PhH, H₂O, 4h, reflux 1b) EtOH, PhH, H₂O, 4.5 h, reflux 2.) 10percent aq. acetone, 2.5 h, 20 deg C

3: 99 percent / DBU / CH₂Cl₂ / 2 h / 0 °C

4: 76 percent / AW-300 molecular sieves, BF₃*Et₂O / 1,2-dichloro-ethane / 2 h / -30 °C

5: NH₂NH₂*H₂O / ethanol / 2 h / Heating

6: pyridine / 1 h / 20 °C

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; molecular sieve; boron trifluoride diethyl etherate; hydrazine hydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide; mercury dichloride; mercury(II) oxide; silver(l) oxide; In ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84224-I

Reference yield:

: 125946-67-0
allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

: 129162-96-5
benzyl O-(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / Ag₂O, KI / dimethylformamide / 4 h / 0 - 20 °C

2: 1.) tris(triphenylphosphine)rhodium(I) chloride, 1,4-diazabicyclo<2.2.2>octane 2.) HgO, HgCl₂ / 1a) EtOH, PhH, H₂O, 4h, reflux 1b) EtOH, PhH, H₂O, 4.5 h, reflux 2.) 10percent aq. acetone, 2.5 h, 20 deg C

3: 99 percent / DBU / CH₂Cl₂ / 2 h / 0 °C

4: 76 percent / AW-300 molecular sieves, BF₃*Et₂O / 1,2-dichloro-ethane / 2 h / -30 °C

5: NH₂NH₂*H₂O / ethanol / 2 h / Heating

6: pyridine / 1 h / 20 °C

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; molecular sieve; boron trifluoride diethyl etherate; hydrazine hydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide; mercury dichloride; mercury(II) oxide; silver(l) oxide; In ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84224-I