1-Propanone,1-phenyl-,oxime,(1E)-(9CI)

Base Information

• Chemical Name: 1-Propanone,1-phenyl-,oxime,(1E)-(9CI)
• CAS No.: 23517-42-2
• Molecular Formula: C9H11 N O
• Molecular Weight: 149.192
• Mol file: 23517-42-2.mol

Synonyms:1-Propanone,1-phenyl-, oxime, (E)-; Propiophenone, oxime, (E)- (8CI); (E)-Propiophenoneoxime; Propiophenone E-oxime

Chemical Property of 1-Propanone,1-phenyl-,oxime,(1E)-(9CI)

Chemical Property:

• Melting Point: 50-51 °C(Solv: hexane (110-54-3))
• Boiling Point: 260.8±9.0 °C(Predicted)
• PKA: 11.35±0.70(Predicted)
• PSA: 32.59000
• Density: 0.99±0.1 g/cm3(Predicted)
• LogP: 2.27490

Purity/Quality:

98%min ^*data from raw suppliers

1-Phenyl-1-propanoneoxime ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Propanone,1-phenyl-,oxime,(1E)-(9CI)

There total 3 articles about 1-Propanone,1-phenyl-,oxime,(1E)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-phenyl-propan-1-one (93-55-0) → propiophenone oxime (23517-42-2)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In methanol; Heating;

DOI:10.1021/jo070297k

Reference yield: 73.0%

[(E)-(2-nitrobut-1-en-1-yl)benzene] (25695-90-3) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → triphenylmethane (519-73-3) + propiophenone oxime (23517-42-2) + 1-phenyl-propan-1-one (93-55-0)

Guidance literature:

With trifluorormethanesulfonic acid; at 0 - 5 ℃; for 6.5h;

DOI:10.1016/S0040-4020(01)89957-9

Reference yield: 53.0%

1-Phenylprop-1-yne (673-32-5) → propiophenone oxime (23517-42-2) + 1-phenylpropan-2-one oxime (13213-36-0)

Guidance literature:

With hydroxylamine; In isopropyl alcohol; at 140 ℃; for 10h; microwave irradiation;

DOI:10.1002/anie.200703495

upstream raw materials:

[(E)-(2-nitrobut-1-en-1-yl)benzene]

benzene

1-phenyl-propan-1-one

1-Phenylprop-1-yne

Downstream raw materials:

N-propylaniline

1-phenylpropylamine

1,1,3,3-tetraphenyldisiloxane

3-[1-Phenyl-prop-(E)-ylideneaminooxy]-propionic acid ethyl ester