chloro(phenylphosphine)dicarbonylbis(triphenylphosphine)osmium(II)perchlorate

Base Information

Chemical Name:chloro(phenylphosphine)dicarbonylbis(triphenylphosphine)osmium(II)perchlorate
CAS No.:102849-35-4
Molecular Formula:C₄₄H₃₇ClO₂OsP₃*ClO₄
Molecular Weight:1015.8
Hs Code.:

Synonyms:chloro(phenylphosphine)dicarbonylbis(triphenylphosphine)osmium(II)perchlorate

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Chemical Property of chloro(phenylphosphine)dicarbonylbis(triphenylphosphine)osmium(II)perchlorate

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Technology Process of chloro(phenylphosphine)dicarbonylbis(triphenylphosphine)osmium(II)perchlorate

There total 1 articles about chloro(phenylphosphine)dicarbonylbis(triphenylphosphine)osmium(II)perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 102849-33-2
chloro(phenylphosphine)(acetonitrile)carbonylbis(triphenylphosphine)osmium(II) perchlorate

: 102849-35-4
chloro(phenylphosphine)dicarbonylbis(triphenylphosphine)osmium(II)perchlorate

Guidance literature:: With carbon monoxide; In dichloromethane; byproducts: CH3CN; High Pressure; treatment of the complex in CH2Cl2 with CO (40 psi) at 25°C for 8 h;; recrystn. from CH2Cl2/i-PrOH; elem. anal.;

Reference yield: 73.0%

: 102849-35-4
chloro(phenylphosphine)dicarbonylbis(triphenylphosphine)osmium(II)perchlorate

: 93366-14-4
Os(PH(OCH₃)(C₆H₅))(CO)2(P(C₆H₅)3)2

Guidance literature:: With CH₃OH; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; N2-atmosphere; dissolving of Os-complex in CH3OH by heating almost to reflux; addn. of DBU; further heating;; cooling to room temp.; crystn. on cooling in ice bath; filtration; washing (MeOH, EtOH, hexane); recrystn. (C6H6/MeOH); elem. anal.;