3-chloropropyl formate

Base Information

• Chemical Name: 3-chloropropyl formate
• CAS No.: 1487-44-1
• Molecular Formula: C₄H₇ClO₂
• Molecular Weight: 122.551
• Mol file: 1487-44-1.mol

Synonyms:3-chloropropyl formate

Chemical Property of 3-chloropropyl formate

Chemical Property:

Purity/Quality:

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Technology Process of 3-chloropropyl formate

There total 1 articles about 3-chloropropyl formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

TETRAHYDROPYRANE (142-68-7) → 2-methyltetrahydrofuran (96-47-9) + Tetrahydro-pyran-4-ol (2081-44-9) + 4-butanolide (96-48-0) + 3,4,5,6-tetrahydro-2H-pyran-2-one (542-28-9,26354-94-9) + Tetrahydro-4H-pyran-4-one (29943-42-8,143562-54-3) + 3-chloropropyl formate (1487-44-1)

Guidance literature:

With clorine; at 24.84 ℃; under 800 Torr; Kinetics; Inert atmosphere; Gas phase;

DOI:10.1002/kin.20765

Reference yield:

ethyleneimine (151-56-4,9002-98-6) + 3-chloropropyl formate (1487-44-1) → 3-(1-Ethylenimino)-1-propanol (31190-87-1)

Guidance literature:

With sodium hydroxide; methyllithium; Yield given. Multistep reaction; 1) Et2O, -15 deg C, 2) Et2O, 5 min, < 10 deg C;

DOI:10.1002/ardp.19923251106

upstream raw materials:

TETRAHYDROPYRANE

Downstream raw materials:

3-(1-Ethylenimino)-1-propanol

Refernces