N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide

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Chemical Name:N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide
CAS No.:1597443-52-1
Molecular Formula:C₂₇H₂₂Br₂N₄O₆S
Molecular Weight:690.369
Hs Code.:

Synonyms:N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide

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Chemical Property of N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide

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Technology Process of N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide

There total 4 articles about N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.5%

: 1597443-58-7
N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide

: 85446-05-5
3,6-dibromo-9-(oxiran-2-ylmethyl)-9H-carbazole

: 1597443-52-1
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide

Guidance literature:: N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide; With n-butyllithium; In hexane; N,N-dimethyl-formamide; at 0 ℃; for 0.25h; Inert atmosphere;

3,6-dibromo-9-(oxiran-2-ylmethyl)-9H-carbazole; In hexane; N,N-dimethyl-formamide; at 80 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jm401919s

Reference yield:

: 17920-35-3
2-amino-6-methoxypyridine

: 1597443-52-1
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / chloroform-d1 / 0.5 h / Cooling with ice; Inert atmosphere

1.2: Cooling with ice; Inert atmosphere

2.1: n-butyllithium / N,N-dimethyl-formamide; hexane / 0.25 h / 0 °C / Inert atmosphere

2.2: 4 h / 80 °C / Inert atmosphere

With pyridine; n-butyllithium; In chloroform-d1; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jm401919s

Reference yield:

: 6825-20-3
3,6-dibromo-9H-carbazole

: 1597443-52-1
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropyl)-N-(6-methoxypyridin-2-yl)-4-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / Inert atmosphere

2.1: n-butyllithium / N,N-dimethyl-formamide; hexane / 0.25 h / 0 °C / Inert atmosphere

2.2: 4 h / 80 °C / Inert atmosphere

With n-butyllithium; potassium hydroxide; In hexane; N,N-dimethyl-formamide;
DOI:10.1021/jm401919s