N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide

Base Information

• Chemical Name: N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide
• CAS No.: 95792-78-2
• Molecular Formula: C₂₂H₃₈NPSe
• Molecular Weight: 426.484
• Mol file: 95792-78-2.mol

Synonyms:N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide

Chemical Property of N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide

There total 2 articles about N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N-tert-butylimino-λ3-2,4,6-tris-(tert-butyl)phenylphosphine (95792-75-9,98039-67-9) → N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide (95792-78-2)

Guidance literature:

With selenium; for 4h; Heating;

DOI:10.1039/c39840001692

Reference yield:

2,4,6-tri-tert-butylphenyllithium (35383-91-6) → N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide (95792-78-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 41 percent / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) 20 deg C, 12 h

2: 65 percent / Se / CH₂Cl₂ / 2 h / 50 °C

With selenium; In tetrahydrofuran; dichloromethane;

Reference yield: 75.0%

methanol (67-56-1) + N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphinimine P-selenide (95792-78-2) → O-methyl N-tert-butyl-P-(2,4,6-tri-tert-butylphenyl)phosphonamidoselenoate

Guidance literature:

In benzene; for 5h;

upstream raw materials:

N-tert-butylimino-λ³-2,4,6-tris-(tert-butyl)phenylphosphine

2,4,6-tri-tert-butylphenyllithium