9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin

Base Information

Chemical Name:9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin
CAS No.:81124-81-4
Molecular Formula:C₂₁H₂₅NO
Molecular Weight:307.436
Hs Code.:

Synonyms:9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin

Suppliers and Price of 9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin

There total 4 articles about 9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 81124-79-0
4-Methyl-1-benzyl-3-<2-(4-methoxyphenyl)ethyl>-1,2,5,6-tetrahydropyridin

: 81124-81-4
9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin

Guidance literature:: With hydrogen bromide; In acetic acid; for 12h; Heating;
DOI:10.1002/ardp.19823150108

Reference yield:

: 72311-19-4
4-Methyl-3-<2-(4-methoxyphenyl)ethyl>pyridin

: 81124-81-4
9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / acetone / 15 h / Ambient temperature

2: aq. NaOH, NaBH₄ / methanol / 0.5 h

3: 71 percent / 48percent HBr / acetic acid / 12 h / Heating

With sodium hydroxide; sodium tetrahydroborate; hydrogen bromide; In methanol; acetic acid; acetone;
DOI:10.1002/ardp.19823150108

Reference yield:

: 100-39-0
benzyl bromide

: 81124-81-4
9-Hydroxy-10-methyl-3-benzyl-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isochinolin

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / acetone / 15 h / Ambient temperature

2: aq. NaOH, NaBH₄ / methanol / 0.5 h

3: 71 percent / 48percent HBr / acetic acid / 12 h / Heating

With sodium hydroxide; sodium tetrahydroborate; hydrogen bromide; In methanol; acetic acid; acetone;
DOI:10.1002/ardp.19823150108