2-(carboxymethyl)-4-iodobenzoic acid

Base Information

Chemical Name:2-(carboxymethyl)-4-iodobenzoic acid
CAS No.:1354742-59-8
Molecular Formula:C₉H₇IO₄
Molecular Weight:306.057
Hs Code.:

Synonyms:2-(carboxymethyl)-4-iodobenzoic acid

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Chemical Property of 2-(carboxymethyl)-4-iodobenzoic acid

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Technology Process of 2-(carboxymethyl)-4-iodobenzoic acid

There total 4 articles about 2-(carboxymethyl)-4-iodobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 408335-76-2
4-amino-2-(carboxymethyl)benzoic acid

: 1354742-59-8
2-(carboxymethyl)-4-iodobenzoic acid

Guidance literature:: 4-amino-2-(carboxymethyl)benzoic acid; With sulfuric acid; sodium nitrite; In water; at -15 - 0 ℃; Inert atmosphere;

With urea; potassium iodide; In water; at -10 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2011.10.058

Reference yield:

: 99-60-5
2-chloro-4-nitrobenzoic acid

: 1354742-59-8
2-(carboxymethyl)-4-iodobenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate; copper(I) bromide / 100 °C / Inert atmosphere

1.2: pH 1

2.1: sodium hydroxide / methanol / 20 °C / Inert atmosphere

2.2: pH 1 / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 2250.23 Torr

4.1: sulfuric acid; sodium nitrite / water / -15 - 0 °C / Inert atmosphere

4.2: -10 - 20 °C / Inert atmosphere

With sulfuric acid; palladium 10% on activated carbon; hydrogen; sodium methylate; copper(I) bromide; sodium hydroxide; sodium nitrite; In methanol; ethanol; water;
DOI:10.1016/j.bmc.2011.10.058

Reference yield:

: 39585-32-5
2-carboxymethyl-4-nitro-benzoic acid

: 1354742-59-8
2-(carboxymethyl)-4-iodobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 2250.23 Torr

2.1: sulfuric acid; sodium nitrite / water / -15 - 0 °C / Inert atmosphere

2.2: -10 - 20 °C / Inert atmosphere

With sulfuric acid; palladium 10% on activated carbon; hydrogen; sodium nitrite; In ethanol; water;
DOI:10.1016/j.bmc.2011.10.058